TECHNICAL SPECIFICATIONS
1. Truncated reactor 50 L
Stainless steel 316 according to industrial standards
Double-walled 6 bars (90 psi) in running
(9 bars (130 psi) possible)
Bottom grid stainless steel 316 L
Rounded cover with charging opening DN 100
2. Liquid supply and dosing tank
Borosilicate glass
Volume : 15 liters
3. Rupture disk
Carbon calibrated at 0.5 bar
4. Agitation modulus single-velocity
ADF type
Agitation velocity 60 R.P.M.
Stainless steel agitator Ψ20 mm with V-cramp for the agitation of the
bottom tank with a low level (5 liters)
5. Couple limiting
Protects the agitation motor against the mass increase of the reaction
medium
6. Light sight
Protection : IP65
7. Distilling column DN 100
Borosilicate glass according to industrial standards
Height : 1000 mm (7 theoretical plates mix of water/methanol)
Multiknit stainless steel padding 1600 m²/m3 Ψ100 mm
8. Condenser
Tubular exchanger : 1 m² (Power = 50 kW)
Calender and chicanes stainless steel 316 L
Diameter : 100 mm
9. Exchanger for distillate
S = 0.2 m2
Tubular type
Glass
10. Azeotropic decanter
Borosilicate glass
Adjustment of the barometric leg with the sliding tube
Double-walled
11. Receiver of the heavy phase of the distillate
Polyethylene
Volume = 20 L
12. Receiver of the light phase of the distillate
Polyethylene
Volume = 20 L
P1 : Centrifugal pump of the hot loop
. stainless steel (316 L) body
. 0-3 m3/h to 3 bar (45 psi)
. P = 0.75 kW |
CHARACTERISTICS
▪ EXPERIMENTAL MEASUREMENTS
▪ TEMPERATURE SENSORS PT 100 STAINLESS STEEL 316 L DIAMETER 6 mm
(T1 to T7)
▪ PRESSURE MEASUREMENT
▪ PRC : Differential pressure sensor P1 P2 P3
▪ FLOW RATE SENSORS
ON THE DISTILLATE (FRC) : Oval-wheel flow meter, pulsed outlet
converted in 4-20 mA
ON THE ARRIVAL OF THE WATER FROM THE CONDENSER (FI 1) : Rotameter
0-1500 L/h
▪ REGULATORS
Heating regulator
Runs with the electrovalves V22 and V24 in
surface sharing
Connected with 3 parameters inter switchable
(TRC1-TRC2-∆PRC)
PID type with microprocessor : class 0.2
Configurable scale, Relay outlet, logic, continuous with proportional band
of 0.5 to 1000 %, integral action time from 0.1 to 100 min, derived action
time from 0.01 to 10 min or self-adaptive for a maximum regulation
Flow back regulator
Regulation of the temperature TRC3 or the distillate flow rate from the
electrovalves on the distillate and the flowiback (V8 and V9) in a surface
sharing working.
PID type with microprocessor : class 0.2
Configurable scale, Relay outlet, logic, continuous with proportional band
of 0.5 to 1000 %, integral action time from 0.1 to 100 min, derived action
time from 0.01 to 10 min or self-adapted for maximum regulation
VALVES
Spherical valves 1/4 - stainless steel
Exceptions :
Vapor arrival valve : stainless steel nozzle valve V31
Water arrival valve : polypropylene spherical valve
Electrovalves V8 V9 V22 V24 : ADF
OPTIONS
- AGITATION MOTOVARIATOR : 60/300 min-1
- HEATING METHOD BY THERMOREGULATOR
Pressurized water thermoregulator :
- Up to 160°C
- Heating power : 15 kW
- Cooling power : 44 kW
- INSTALLATION IN ADF
- COMPUTERIZATION |
